Triethylamine → HCID 53795161, compound

HRID 1658915Notes

Reaction equation

HRID 1658915 reaction equation
[O:1]1[NH:10][CH2:9][CH2:8][O:7][CH2:6][CH2:5][NH:4][CH2:3][CH2:2]1.[CH2:11](N(CC)CC)[CH3:12].Cl[C:19]([CH2:21][O:22][C:23]1[CH:28]=[CH:27][CH:26]=[CH:25][C:24]=1[O:29][CH2:30][C:31](Cl)=[O:32])=[O:20]>C1C=CC=CC=1>[O:20]=[C:19]1[CH2:21][O:22][C:23]2[C:24](=[CH:25][CH:26]=[CH:27][CH:28]=2)[O:29][CH2:30][C:31](=[O:32])[N:10]2[CH2:9][CH2:8][O:7][CH2:6][CH2:5][N:4]1[CH2:3][CH2:2][O:1][CH2:11][CH2:12]2

Participants

5

Reactant 3

HCID 8471TriethylamineHCID 11076276Acetyl chloride, 2,2'-[1,2-phenylenebis(oxy)]bis-2×HCID 21316300HCID 21316300, compound

Product 1

HCID 53795161HCID 53795161, compound

Reagents, catalysts & solvents 1

HCID 241BenzeneSolvent

Procedure

In a manner similar to that described in Example 5, treat the cyclic diamine obtained in Example 45 and triethylamine in anhydrous benzene with 1,2-di-(chlorocarbonylmethoxy)-benzene (compound of Example 61) utilizing high dilution technique. Isolate and purify the resultant product in a manner similar to that described in Example 5 to obtain 2,13-dioxo-4,11,17,22-tetraoxa-1,14-diaza-tricyclo[12,5,5,05,10 ]tetracosa-5,7,9-triene.

Workup

  1. customIsolate
  2. custompurify the resultant product in a manner similar to

Sources & evidence

ORD record
ord-3c61811b6ab046b18a2238f9d8635461
Source dataset
uspto-grants-1976_06
Patent number
US03966766

Reaction notes

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