2-Methoxyethylamine → 3,5-Dinitro-4-[2-methoxyethyl-amino]-2-chlorobenzotrifluoride

HRID 1658950Notes

Reaction equation

HRID 1658950 reaction equation
[CH3:1][O:2][CH2:3][CH2:4][NH2:5].[Cl:6][C:7]1[C:12]([N+:13]([O-:15])=[O:14])=[C:11](Cl)[C:10]([N+:17]([O-:19])=[O:18])=[CH:9][C:8]=1[C:20]([F:23])([F:22])[F:21]>C1CCCCC1>[CH3:1][O:2][CH2:3][CH2:4][NH:5][C:11]1[C:10]([N+:17]([O-:19])=[O:18])=[CH:9][C:8]([C:20]([F:21])([F:22])[F:23])=[C:7]([Cl:6])[C:12]=1[N+:13]([O-:15])=[O:14]

Participants

4

Reactant 2

HCID 80182-MethoxyethylamineHCID 943982,4-Dichloro-1,3-dinitro-5-(trifluoromethyl)benzene

Product 1

HCID 205718683,5-Dinitro-4-[2-methoxyethyl-amino]-2-chlorobenzotrifluoride

Reagents, catalysts & solvents 1

HCID 8078CyclohexaneSolvent

Procedure

The compound was prepared by reacting 2-methoxyethylamine was 2,4-dichloro-3,5-dinitrobenzotrifluoride in cyclohexane to give the product melting at 106.5° - 107.5°C.

Workup

  1. customThe compound was prepared

Sources & evidence

ORD record
ord-0a1b8ea17687445da40887b5df67ae38
Source dataset
uspto-grants-1976_06
Patent number
US03966816

Reaction notes

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