Diethylamine → Benzenamine, 3-chloro-N,N-diethyl-2,6-dinitro-4-(trifluoromethyl)-

HRID 1658952Notes

Reaction equation

HRID 1658952 reaction equation
[CH2:1]([NH:3][CH2:4][CH3:5])[CH3:2].[Cl:6][C:7]1[C:12]([N+:13]([O-:15])=[O:14])=[C:11](Cl)[C:10]([N+:17]([O-:19])=[O:18])=[CH:9][C:8]=1[C:20]([F:23])([F:22])[F:21]>C(O)C>[CH2:1]([N:3]([CH2:4][CH3:5])[C:11]1[C:10]([N+:17]([O-:19])=[O:18])=[CH:9][C:8]([C:20]([F:23])([F:22])[F:21])=[C:7]([Cl:6])[C:12]=1[N+:13]([O-:15])=[O:14])[CH3:2]

Participants

4

Reactant 2

HCID 8021DiethylamineHCID 943982,4-Dichloro-1,3-dinitro-5-(trifluoromethyl)benzene

Product 1

HCID 118978Benzenamine, 3-chloro-N,N-diethyl-2,6-dinitro-4-(trifluoromethyl)-

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

The compound was prepared by reacting diethylamine with 2,4-dichloro-3,5-dinitrobenzotrifluoride in ethanol to give the product melting at 35° - 36°C.

Workup

  1. customThe compound was prepared

Sources & evidence

ORD record
ord-021de5c8457247578ece21793f2f21ba
Source dataset
uspto-grants-1976_06
Patent number
US03966816

Reaction notes

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