HCID 178442626, compound → HCID 178442627, compound

HRID 1658997Notes

Reaction equation

HRID 1658997 reaction equation
[C:1]([C:4](C(O)=O)([CH2:16][CH3:17])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]1[C:11](=[O:15])[CH2:12][CH2:13][CH:14]=1)([OH:3])=[O:2].[CH:21]1[C:22](/[CH:37]=[N:38]/[OH:39])=[CH:23][CH:24]=[N+:25]([CH2:27][N+:28]2[CH:33]=[CH:32][C:31](/[CH:34]=[N:35]/[OH:36])=[CH:30][CH:29]=2)[CH:26]=1.[Br-:40].[Br-]>C1(C)C(C)=CC=CC=1>[C:1]([CH:4]([CH2:16][CH3:17])[CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][C:10]1[C:11](=[O:15])[CH2:12][CH2:13][CH:14]=1)([OH:3])=[O:2].[CH:23]1[C:22](/[CH:37]=[N:38]/[OH:39])=[CH:21][CH:26]=[N+:25]([CH2:27][N+:28]2[CH:29]=[CH:30][C:31](/[CH:34]=[N:35]/[OH:36])=[CH:32][CH:33]=2)[CH:24]=1.[Br-:40].[Br-:40]

Participants

3

Reactant 1

HCID 178442626HCID 178442626, compound

Product 1

HCID 178442627HCID 178442627, compound

Reagents, catalysts & solvents 1

HCID 7237O-XyleneSolvent

Procedure

In the manner described in Example 21, treatment of 2-(6,6-dicarboxyoctyl)-2-cyclopentenone methoxime (Example 28) with xylene at reflux for 18 hours gives a yellow oil.

Workup

  1. temperatureat reflux for 18 hours
  2. customgives a yellow oil

Sources & evidence

ORD record
ord-b8b9fd4b94094f2aa38b295843df92d6
Source dataset
uspto-grants-1976_06
Patent number
US03966773

Reaction notes

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