HRID1659065

反应详情

EQUATION

反应方程式

HRID 1659065 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A suspension of 100 g of p-(2-chlorophenyl)cinnamic acid in 1 l. of 95% ethanol is hydrogenated at atmospheric pressure using platinum oxide catalyst (1 g). The uptake of hydrogen ceases when approximately 9-10 l. of hydrogen is consumed. The catalyst is then filtered off and the reaction evaporated to dryness to give β-(2'-chloro-4-biphenylyl)propionic acid.

WORKUP

后处理

  1. customof hydrogen is consumed
  2. filtrationThe catalyst is then filtered off
  3. customthe reaction evaporated to dryness