HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 21526359, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 21526381 | HCID 21526381 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 21526359 | HCID 21526359 | — |
Reaction Steps
To a solution of 0.01 moles of ethyl α-hydroxy-γ-(3-amino-4-cyclohexylphenyl)butyrate in 100 ml. of pyridine is added 0.1 moles of methyl iodide. The reaction mixture is stirred overnight at room temperature, filtered and concentrated. The residue is distilled to obtain ethyl α-hydroxy-γ-(3-methylamino -4-cyclohexylphenyl)butyrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03966801 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-946e59d4561f491bb848efccc44aba85 |
| Source note | uspto-grants-1976_06 |