HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 21526455, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 21526370 | HCID 21526370 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 21526455 | HCID 21526455 | — |
Reaction Steps
A solution of 0.01 moles of benzyl α-hydroxy-γ-(3-cyano-4-cyclohexylphenyl)butyrate dissolved in 100 ml. of acetic acid and containing 0.01 mole of hydrogen chloride is shaken with hydrogen over a 5% Pd carbon catalyst until 0.01 moles of hydrogen is absorbed. The catalyst is then filtered and the solution is evaporated to dryness and crystallized to obtain α-hydroxy-γ-(3-cyano-4-cyclohexylphenyl)butyric acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03966801 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-82cc959c4f1e4dd0ad4dee2c24c1b75a |
| Source note | uspto-grants-1976_06 |