HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 86733634, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Ethyl orthopropionate | HCID 66995 | — |
| Reactant | N-Phenylrhodanine | HCID 73822 | — |
| Product | HCID 86733634 | HCID 86733634 | — |
Reaction Steps
A mixture of 8.4 g. (0.04 m.) of 3-phenylrhodanine, 21 g. (0.12 m.) of triethylorthopropionate and 80 ml. of acetic anhydride is heated under reflux for six hours, cooled and filtered. The solid is washed with 50% aqueous acetic acid to afford 5-(1'-ethoxypropylidene)-3-phenylrhodanine, m.p. 178°-181°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03966942 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-25d833ba28b94deb89be58210eb699b1 |
| Source note | uspto-grants-1976_06 |