HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Anhydride → HCID 178467560, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Anhydride | HCID 7918 | — |
| Reactant | Rhodanine | HCID 1201546 | — |
| Reactant | Triethylorthoaceate | HCID 21875354 | — |
| Reactant | HCID 86733635 | HCID 86733635 | — |
| Product | HCID 178467560 | HCID 178467560 | — |
Reaction Steps
Similar reaction of this rhodanine (0.2 m.) with 140 g. (0.86 m.) of triethylorthoacetate in 350 ml. of acetic anhydride followed by alkaline hydrolysis of the intermediate 5-(1'-ethoxyethylidene)-3-(4'-fluorophenyl)-rhodanine gives the corresponding 3-(4'-fluorophenyl)-5-(1'-hydroxyethylidene)-rhodanine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03966942 |
| Source dataset | uspto-grants-1976_06 |
| ORD ID | ord-1c17c06393fe4356abc6e457691db2fb |
| Source note | uspto-grants-1976_06 |