HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetone → HCID 135737780, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetone | HCID 180 | — |
| Reactant | 5-(o-Aminophenyl)-4-nitropyrazole | HCID 20560260 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 135737780 | HCID 135737780 | — |
Reaction Steps
A mixture of 20.4 g (0.1 mole) of 5-(o-aminophenyl)-4-nitropyrazole, 300 ml of acetone and 0.3 ml of acetic acid is heated under reflux for 1 hour. After evaporation, 24.0 g (98.5%) of 1-nitro-5,5-dimethyl-5,6-dihydropyrazolo[1,5-c]quinazoline are obtained. M.p.: 193°-195° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04303660 |
| Source dataset | uspto-grants-1981_12 |
| ORD ID | ord-fec0379702d540f6b1abab26cb1f9859 |
| Source note | uspto-grants-1981_12 |