4-Aminobenzoic Acid → HCID 86738145, compound

HRID 1659443Notes

Reaction equation

HRID 1659443 reaction equation
[Si:1]([O-:5])([O-:4])([O-:3])[O-:2].[Na+:6].[Na+].[Na+].[Na+].NC1C=CC(C(O)=O)=CC=1.S([O-])(OCCCCCCCCCCCC)(=O)=O.[Na+].C(OOC(=O)C)(=O)C.C(OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1.[C:64]([Cl:67])([Cl:66])=[CH2:65]>>[Si:1]([O-:5])([O-:4])([O-:3])[O-:2].[Na+:6].[Na+:6].[Na+:6].[Na+:6].[C:64]([Cl:67])([Cl:66])=[CH2:65]

Participants

7

Reactant 6

HCID 9784-Aminobenzoic AcidHCID 6366Vinylidene chlorideHCID 7187Benzoyl PeroxideHCID 8040Peroxide, diacetylHCID 26051Sodium orthosilicateHCID 3423265Sodium Lauryl Sulfate

Product 1

HCID 86738145HCID 86738145, compound

Procedure

About 50 parts by weight of an aqueous sodium silicate solution containing about 14.7% Na2O and 29.4% SiO2 by weight, 2 parts by weight of para-aminobenzoic acid, 0.5 parts by weight of sodium lauryl sulphate, 0.05 parts by weight acetyl peroxide, 0.05 parts by weight of benzoyl peroxide and 30 parts by weight of vinylidene chloride are mixed thoroughly thereby forming a stable emulsion. The mixture is polymerized in 1 to 24 hours thereby producing a poly(sodium silicate-vinylidene chloride copolymer emulsion).

Workup

  1. additionare mixed thoroughly
  2. customthereby forming a stable emulsion
  3. customThe mixture is polymerized in 1 to 24 hours

Sources & evidence

ORD record
ord-1d3ee778862f4ec9906481c5fd668026
Source dataset
uspto-grants-1981_12
Patent number
US04303768

Reaction notes

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