Water → HCID 20559067, compound

Participants

Reaction Steps

The procedure of Example 1 was repeated using dimethyldisulphide (96 mg; 1.02 mmol) and 1-hexane (670 mg: 8 mmol) in acetonitrile (15 ml) at +1.20 V until 1.3 coulomb equivalents of charge had been passed. After the addition of water and extraction with diethyl ether there was obtained 36 mg of 2-acetamido-1-methylthio-hexane. Mass Spec. m/e 189 (M+), 130 (57%) and 86 (100%). I.R. 3290 & 1645 cm-1.

Provenance & Evidence