HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cysteamine Hydrochloride → HCID 131712297, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cysteamine Hydrochloride | HCID 9082 | — |
| Reactant | HCID 20559455 | HCID 20559455 | — |
| Solvent | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 131712297 | HCID 131712297 | 125.9% |
Reaction Steps
5-[[Hydroxy(methyl)amino]methyl]-2-furanmethanol (7.85 g) was added to a stirred solution of 2-aminoethanethiol hydrochloride (5.68 g) in concentrated hydrochloric acid (15 ml) at 0° during 45 mins. After 48 hr at 0° the crystalline solid which separated was mixed with isopropanol (40 ml), filtered and crystallised from ethanol to give the title compound (9.1 g) m.. 164°-165° dec.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04304780 |
| Source dataset | uspto-grants-1981_12 |
| ORD ID | ord-199b78c34d2946c193d5f26aa1a8cfc7 |
| Source note | uspto-grants-1981_12 |