HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzhydrylamine → HCID 12805911, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzhydrylamine | HCID 7036 | — |
| Reactant | 1,3-Dibromobutane | HCID 7889 | — |
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 12805911 | HCID 12805911 | — |
Reaction Steps
Combine benzhydrylamine (27.5 g=0.15 ml), 1,3-dibromobutane (40.5 g=0.19 mol) and sodium carbonate (28 g=0.33 mol) in 250 ml acetonitrile. Reflux 24 hours, allow to cool, filter and concentrate. Dissolve the residue in ether and wash with 1% sodium carbonate solution. Dry, concentrate and distill to obtain the product, boiling point 110°-115° C./0.1 mm pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04304790 |
| Source dataset | uspto-grants-1981_12 |
| ORD ID | ord-b4f93fd6d287430091cacabf4e57c9de |
| Source note | uspto-grants-1981_12 |