HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12520066, compound → 3-Isopropyl-5-(2-hydroxy-styryl)-isoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12520066 | HCID 12520066 | — |
| Reactant | Diethyl (3-isopropyl-isoxazol-5-yl)methanephosphonate | HCID 12520069 | — |
| Product | 3-Isopropyl-5-(2-hydroxy-styryl)-isoxazole | HCID 136081920 | — |
Reaction Steps
Using the method described in Example I, 32 g (0.12 mole) of diethyl (3-isopropyl-isoxazol-5-yl)methanephosphonate and 22 g (0.12 mole) of o-(1-methoxy-ethoxy)-benzaldehyde are reacted and the product is recrystallized from toluene. 20 g (73% of theory) of colorless crystals, of melting point 129°-133° C., are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04305951 |
| Source dataset | uspto-grants-1981_12 |
| ORD ID | ord-e63477f61b1b4bc8bbd3a9ae184df4aa |
| Source note | uspto-grants-1981_12 |