HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 12520066, compound → 3-Tert.-butyl-5-(2-hydroxystyryl)-isoxazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 12520066 | HCID 12520066 | — |
| Reactant | Diethyl (3-tert.-butyl-isoxazol-5-yl)methanephosphonate | HCID 12520070 | — |
| Product | 3-Tert.-butyl-5-(2-hydroxystyryl)-isoxazole | HCID 135973981 | — |
Reaction Steps
Using the method described in Example I, 35 g (0.13 mole) of diethyl (3-tert.-butyl-isoxazol-5-yl)methanephosphonate and 23 g (0.13 mole) of o-(1-methoxy-ethoxy)-benzaldehyde are reacted and the product is recrystallized from toluene. 24.8 g (78% of theory) of colorless crystals, of melting point 152°-155° C., are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04305951 |
| Source dataset | uspto-grants-1981_12 |
| ORD ID | ord-0a397829661e49778604a3bc534a9753 |
| Source note | uspto-grants-1981_12 |