Acetone → HCID 86736124, compound

HRID 1659974Notes

Reaction equation

HRID 1659974 reaction equation
[C:1]1(=[O:7])[O:6][C:4](=[O:5])[CH:3]=[CH:2]1.[OH-].[Li+:9].C[C:11](C)=[O:12]>CO>[C:4]([O:12][CH3:11])(=[O:5])/[CH:3]=[CH:2]\[C:1]([O-:6])=[O:7].[Li+:9]

Participants

5

Reactant 3

HCID 180AcetoneHCID 3939Lithium Hydroxide2×HCID 7923Maleic Anhydride

Product 1

HCID 86736124HCID 86736124, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Twenty grams of maleic anhydride is dissolved in 200 mis methanol, 4.8 grams (0.2 moles) lithium hydroxide is added. The mixture is stirred until all the lithium hydroxide dissolves (at this point the pH reads 7.0). To the solution is added acetone and the solid is filtered and dried. 23 grams product is obtained.

Workup

  1. additionis added
  2. dissolutiondissolves (at this point the pH
  3. filtrationthe solid is filtered
  4. customdried

Sources & evidence

ORD record
ord-18b67878806741f2ab4929690d7a7f4c
Source dataset
uspto-grants-1981_12
Patent number
US04306079

Reaction notes

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