HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Thionyl Chloride → 8-Methoxy-1,4-benzodioxane-5-carbonyl chloride
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Thionyl Chloride | HCID 24386 | — |
| Edukt | 8-Methoxy-2,3-dihydrobenzo[b][1,4]dioxine-5-carboxylic Acid | HCID 22734248 | — |
| Produkt | 8-Methoxy-1,4-benzodioxane-5-carbonyl chloride | HCID 20544710 | 100,6% |
Reaktionsschritte
391 g of thionyl chloride and 138 g of 8-methoxy-1,4-benzodioxane-5-carboxylic acid were introduced into a balloon flask provided with a condenser. The mixture was heated to 50°-55° C. and the excess thionyl chloride was distilled off under vacuum. 151 g of 8-methoxy-1,4-benzodioxane-5-carbonyl chloride were obtained (yield: 100%).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04306072 |
| Quelldatensatz | uspto-grants-1981_12 |
| ORD ID | ord-92993792b1a942c2907a131ffdc84638 |
| Quellennotiz | uspto-grants-1981_12 |