HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Dichloroacetone → HCID 131712621, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Dichloroacetone | HCID 10793 | — |
| Reactant | (+-)-alpha-(2,4-Dichlorophenyl)-1H-imidazole-1-ethanol | HCID 32238 | — |
| Reactant | 4-(Chloromethyl)-2-phenyl-1,3-thiazole | HCID 236969 | — |
| Reactant | Thiobenzamide | HCID 683563 | — |
| Product | HCID 131712621 | HCID 131712621 | — |
Reaction Steps
Following the procedure of Example 1b, 4-chloromethyl-2-phenylthiazole (prepared according to Example 1a from thiobenzamide and 1,3-dichloroacetone, m.p. 134°-136° C. (absolute alcohol/ethylacetate), is reacted with 1-(2,4-dichlorophenyl)-2-(1H-imidazol-1-yl)ethanol to obtain the title compound, m.p. 204°-205° C. (absolute alcohol/ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04307105 |
| Source dataset | uspto-grants-1981_12 |
| ORD ID | ord-51ec89eeee164a9d8824acfede225fd2 |
| Source note | uspto-grants-1981_12 |