HRID1660483

反应详情

EQUATION

反应方程式

HRID 1660483 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

4.4 parts by weight of phosphonoformic acid hydrazide are run in 20 parts by volume of water and neutralised by a 2 molar solution of diethanol amine in water. The resulting solution is evaporated, the evaporation residue is triturated with a mixture of ethanol and methanol (90 parts by volume plus 10 parts by volume) and the crystals are isolated 11 parts by weight of diethanol ammonium salt of phosphonoformic acid hydrazide are obtained (yield 100%).

WORKUP

后处理

  1. customThe resulting solution is evaporated
  2. customthe evaporation residue is triturated with a mixture of ethanol and methanol (90 parts by volume plus 10 parts by volume)