HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfur trioxide → 2-(4-Methylphenyl)-2-sulphoacetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfur trioxide | HCID 24682 | — |
| Reactant | 2-(4-Methylphenyl)acetyl chloride | HCID 2760634 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-(4-Methylphenyl)-2-sulphoacetyl chloride | HCID 20556805 | — |
Reaction Steps
A solution of 4-methylphenylacetyl chloride (1.69 g, 10 mmole) in dichloromethane (20 ml) was treated with a suspension of sulphur trioxide--dioxane complex (15 mmole) in dichloromethane. The mixture was stirred at room temperature for eighteen hours and evaporated.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04308259 |
| Source dataset | uspto-grants-1981_12 |
| ORD ID | ord-35d560aac5b84defb7eaee8375b6e182 |
| Source note | uspto-grants-1981_12 |