HRID1660541

反应详情

EQUATION

反应方程式

HRID 1660541 的结构方程式

PROCEDURE

实验过程

2,2-Bis(3-allyl-4-hydroxyphenyl)propane (1 mole) was mixed with potassium hydroxide pellets (2.2 moles) and the mixture was stirred and heated at 110° for 30 minutes. The mixture was cooled, neutralised with dilute hydrochloric acid, and the product was extracted to give methylene chloride. The solution was dried and evaporated to give substantially pure 2,2-bis(3-(1-propenyl)-4-hydroxyphenyl)propane.

WORKUP

后处理

  1. temperatureheated at 110° for 30 minutes
  2. temperatureThe mixture was cooled
  3. extractionthe product was extracted
  4. customto give methylene chloride
  5. customThe solution was dried
  6. customevaporated