HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 131712261, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Hexane | HCID 8058 | — |
| Reactant | Hypochlorous Acid | HCID 24341 | — |
| Reactant | Dihydro-alpha-ionone | HCID 35821 | — |
| Product | HCID 131712261 | HCID 131712261 | 59% |
Reaction Steps
The reaction of α-dihydro-ionone and hypochlorous acid was carried out as described in Example 1 except that hexane was substituted for methylene chloride. A 59% yield of 4-(5-chloro-6-methylene-2,2-dimethylcyclohexyl-2-butanone was obtained. The spectral data was identical to that reported in Example 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04308401 |
| Source dataset | uspto-grants-1981_12 |
| ORD ID | ord-116bf892051c412385583456dc846fa6 |
| Source note | uspto-grants-1981_12 |