HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isopropanol → HCID 25056266, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isopropanol | HCID 3776 | — |
| Reactant | L-Tartaric acid | HCID 444305 | — |
| Reactant | Evogliptin | HCID 25022354 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Water ethanol | HCID 19096565 | — |
| Product | HCID 25056266 | HCID 25056266 | 101.9% |
Reaction Steps
55 mg of the compound obtained in Example 11 was dissolved in 0.56 mL of acetone to which a solution of 26 mg of L-tartaric acid in 0.35 mL of ethanol/water (9/1(v/v)) was then slowly added, followed by stirring for 30 min. 0.56 mL of 2-propanol was added thereto, followed by stirring for 10 min and filtration to afford 77 mg of the title compound as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08030315B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-4a7e0fe50e384fd4a0b6b750e59b48db |
| Source note | uspto-grants-2011_10 |