HuagongsheHuagongshe Chemistry Print Report · For research reference only
Succinic Acid → HCID 25056528, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Succinic Acid | HCID 1110 | — |
| Reactant | Evogliptin | HCID 25022354 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Propan-2-one--water (1/1) | HCID 18366337 | — |
| Product | HCID 25056528 | HCID 25056528 | 92.5% |
Reaction Steps
498 mg of the compound obtained in Example 11 was dissolved in 3 mL of acetone to which a solution of 147 mg of succinic acid in 2 mL of acetone/water (20/1(v/v)) was then slowly added followed by stirring for 30 min. The reaction mixture was concentrated to dryness under reduced pressure to afford 596 mg of the title compound as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08030315B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-16cd98bd1838462695072ee019017a26 |
| Source note | uspto-grants-2011_10 |