HuagongsheHuagongshe Chemistry Print Report · For research reference only
(3-Bromophenyl)boronic acid → HCID 59864214, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (3-Bromophenyl)boronic acid | HCID 2734318 | — |
| Reactant | HCID 59864171 | HCID 59864171 | — |
| Solvent | Ethyl acetate hexane | HCID 21226206 | — |
| Product | HCID 59864214 | HCID 59864214 | — |
Reaction Steps
The title compound is prepared as described in Ex. 3 (Step 3.1) for 1-(3′-chloro-2-trifluoromethyl-biphenyl-4-yl)-3-{4-[2-(4-dimethylamino-butylamino)-pyrimidin-4-yloxy]-2-methyl-phenyl}-urea but using 3-bromophenylboronic acid (Aldrich). The title compound: MS: 315.9 [M-1]−; HPLC DtRet=4.9; Rf=0.16 (Hexane/EtOAc, 4:1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08030311B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-d6c2e87c82af41bab997d3843bbcf533 |
| Source note | uspto-grants-2011_10 |