HCID 67021390, compound → HCID 67021578, compound

Participants

Reaction Steps

10% Pd/C (9 mg) is added to a solution of [4-(3-nitro-pyridin-2-ylamino)-phenyl]oxo-acetic acid ethyl ester (26 7 mg, 0.847 mmol) in ethanol (2 mL). The mixture is stirred at rt for 1.5 h under H2. The reaction mixture is filtered through celite and the solvent removed under vacuum to afford [4-(3-amino-pyridin-2-ylamino)-phenyl]oxo-acetic acid ethyl ester as a yellow solid. Title compound: ES-MS: 286.10 [M+H]+; tR=0.9 min (System 2).

Provenance & Evidence