HuagongsheHuagongshe Chemistry Print Report · For research reference only
AP-24592 → HCID 67021656, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | AP-24592 | HCID 46838908 | — |
| Reactant | (4-Imidazo[4,5-b]pyridin-3-yl-2-methyl-phenyl)-acetic acid | HCID 67021622 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 67021656 | HCID 67021656 | — |
Reaction Steps
The title compound is prepared as described in Example 7 but using (4-imidazo[4,5-b]pyridin-3-yl-2-methyl-phenyl)-acetic acid (Step 60.1) and 4-(4-methyl-piperazin-1-ylmethyl)-3-trifluoromethyl-phenylamine (disclosed in WO 03/099771). Title compound: ES-MS: 523.0 [M+H]+; tR=3.11 min (System 1); Rf=0.18 (CH2Cl2/MeOH, 95:5+0.1% NH3aq).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08030311B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-c2cd1cce6a8a49669e5799f9053115af |
| Source note | uspto-grants-2011_10 |