HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl isothiocyanate → HCID 178432727, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl isothiocyanate | HCID 11167 | — |
| Reactant | 2,4-Dimethylthiazole-5-carbohydrazide | HCID 2743669 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178432727 | HCID 178432727 | 47.6% |
Reaction Steps
To a 2,4-dimethylthiazole-5-carbohydrazide (Prep26, 23 g, 0.13 mol) in ethanol (100 ml), methyl isothiocyanate (49.1 g, 0.67 mol) was added. The mixture was refluxed overnight. Then the ethanol was partially removed under vacuum and the residue was filtered. The solid was dried under vacuum to afford 14 g of the title compound (y=46%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08030322B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-6a53f4a191fd4b9688199acb32574d83 |
| Source note | uspto-grants-2011_10 |