Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Cyanide | HCID 9032 | — |
| Reactant | HCID 68217632 | HCID 68217632 | — |
| Solvent | Ethanol | HCID 702 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 59233930 | HCID 59233930 | — |
Reaction Steps
To a solution of (E)-ethyl 2-cyano-2-(6-fluoro-2,3-dihydro-1H-inden-1-ylidene)acetate (Prep44, 7.5 g, 0.03 mol) in ethanol (100 ml), a solution of KCN (4.65 g, 0.08 mol) in water (30 ml) was added. The mixture was warmed to 65° C., and stirred for 7 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08030322B2 |
|---|
| Source dataset | uspto-grants-2011_10 |
|---|
| ORD ID | ord-bb6e6be71c764db59dfdccb83f26dbc8 |
|---|
| Source note | uspto-grants-2011_10 |
|---|
