HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Fluorobenzoyl chloride → HCID 3486255, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Fluorobenzoyl chloride | HCID 74376 | — |
| Reactant | HCID 46737061 | HCID 46737061 | — |
| Solvent | Dichloromethane methanol | HCID 21226129 | — |
| Product | HCID 3486255 | HCID 3486255 | 53% |
Reaction Steps
The compound was prepared following the procedure described in the Example 3 (D), using 3-Fluoro-benzoyl chloride as the acyl chloride of choice and the 3-(3-Phenyl-[1,2,4]oxadiazol-5-yl)-piperidine hydrochloride (already prepared before in the Example 7). Yield: 53% (yellow oil); Rf=0.25 (DCM/MeOH:98/2); LCMS (Tr): 4.77 min (Method C); MS (ES+) gave m/z: 352.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08030331B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-3c2f6cd4d0004a359ecb444191cc249d |
| Source note | uspto-grants-2011_10 |