HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 86634424, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 16128907 | HCID 16128907 | — |
| Product | HCID 86634424 | HCID 86634424 | — |
Reaction Steps
A solution of 10a (2.0 g, 7.6 mmol) in oxalyl chloride (30 ml) was stirred at 60° C. overnight. Excess oxalyl chloride was removed under reduced pressure to leave 11a.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08030339B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-8d43afc4219e40f18e6c093f25feee0e |
| Source note | uspto-grants-2011_10 |