HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57706140, compound → HCID 57705681, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57706140 | HCID 57706140 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 57705681 | HCID 57705681 | 99.6% |
Reaction Steps
To a stirred solution of 78.8A (0.291 g, 0.86 mmol) in EtOAc (2.00 mL) at 23° C. was added palladium on carbon (0.092 g, 0.86 mmol). The reaction was placed under an atmosphere of hydrogen and stirred for four hours. The reaction was then concentrated in vacuo to yield 78.8B (0.290 g, 99% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08030354B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-b933f304257f4789b85ef4bc70064168 |
| Source note | uspto-grants-2011_10 |