HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21925466, compound → HCID 67428844, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21925466 | HCID 21925466 | — |
| Reactant | 4-Methoxy-2-(trifluoromethoxy)benzene sulfonyl chloride | HCID 86625684 | — |
| Product | HCID 67428844 | HCID 67428844 | 88.2% |
Reaction Steps
With 1.50 g of tert-butyl N-[5-chloro-3-(2-methoxyphenyl)-2-oxo-2,3-dihydro-1H-indol-3-yl]-β-alaninate, which is the compound described in Preparation 1.29A of the brochure Publication No. WO03/008407, and 1.15 g of 4-methoxy-2-(trifluoromethoxy)benzene sulfonyl chloride as starting materials, 2.13 g of the title compound (light yellow solid) was obtained by a similar method to Example 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08030499B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-100ee27e584d45afbacd8e7d46dbfdf6 |
| Source note | uspto-grants-2011_10 |