HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67427843, compound → HCID 59867901, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67427843 | HCID 67427843 | — |
| Reactant | 4-Methoxy-2-(trifluoromethoxy)benzene sulfonyl chloride | HCID 86625684 | — |
| Product | HCID 59867901 | HCID 59867901 | — |
Reaction Steps
With 0.88 g of the compound obtained in Step 65-3 and 0.649 g of 4-methoxy-2-(trifluoromethoxy)benzene sulfonyl chloride as starting materials, respectively 140 mg (Isomer A, colorless amorphous) and 170 mg (Isomer B, colorless amorphous) of two species of diastereoisomers of the title compound were obtained by a similar method to Example 2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08030499B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-8742d8f3ec5c44fd94c8ec3dc2d21227 |
| Source note | uspto-grants-2011_10 |