1-Bromonaphthalene → HCID 49765701, compound

HRID 1662770Notes

Reaction equation

HRID 1662770 reaction equation
[C:1]1(Br)[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1.[Cl:12][C:13]1[CH:14]=[C:15]2[C:19](=[CH:20][CH:21]=1)[NH:18][C:17](=[O:22])[C:16]2=[O:23]>>[Cl:12][C:13]1[CH:14]=[C:15]2[C:19](=[CH:20][CH:21]=1)[NH:18][C:17](=[O:22])[C:16]2([OH:23])[C:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 70011-BromonaphthaleneHCID 872035-chloro-1H-indole-2,3-dione

Product 1

HCID 49765701HCID 49765701, compound

Procedure

With 2.81 g of 1-naphthyl bromide 4.34 g, 5-chloroisatin as starting material, 4.30 g of the title compound (yellow solid) was obtained by a similar method to Step 21-1.

Sources & evidence

ORD record
ord-82b428e8898d4bbebf9eb42da42b8bc6
Source dataset
uspto-grants-2011_10
Patent number
US08030499B2

Reaction notes

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