2-Bromonaphthalene → HCID 67429202, compound

HRID 1662799Notes

Reaction equation

HRID 1662799 reaction equation
Br[C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH:3]=1.[Cl:12][C:13]1[CH:14]=[C:15]2[C:19](=[CH:20][CH:21]=1)[NH:18][C:17](=[O:22])[C:16]2=[O:23]>>[Cl:12][C:13]1[CH:14]=[C:15]2[C:19](=[CH:20][CH:21]=1)[NH:18][C:17](=[O:22])[C:16]2([OH:23])[C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[CH:3]=1

Participants

3

Reactant 2

HCID 113722-BromonaphthaleneHCID 872035-chloro-1H-indole-2,3-dione

Product 1

HCID 67429202HCID 67429202, compoundYield 91.6%

Procedure

With 11.1 g of 2-bromonaphthalene and 5.00 g of 5-chloroisatin as starting materials, 7.81 g of the title compound was obtained by a similar method to Step 21-1.

Sources & evidence

ORD record
ord-68d81175b7224adab2d0d199a83d64f2
Source dataset
uspto-grants-2011_10
Patent number
US08030499B2

Reaction notes

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