HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10114725, compound → HCID 178436576, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10114725 | HCID 10114725 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 178436576 | HCID 178436576 | — |
Reaction Steps
In analogy to Ex. 1, 500 mg (1.11 mMol) of 1-(3-bromo-4-ethyl-anilino)-4-[2-methoxy-(pyridin-4-yl)-methyl]-phthalazine in 12 ml of chloroform are reacted with 0.3 ml (2.2 mMol) Me3Sil to give the title compound: M.p. 251-252° C.; FAB-MS: (M+H)+=435/437; HPLC(Grad20-100) tRet=9.6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08034814B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-708360d0e3db49f6950a55b899269807 |
| Source note | uspto-grants-2011_10 |