HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 21096913, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | HCID 21096914 | HCID 21096914 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 21096913 | HCID 21096913 | — |
Reaction Steps
2.20 ml (30.10 mmol) of thionyl chloride are added dropwise to a solution of 3.09 g (12.10 mmol) of 2-[1-(1-isoquinolyl)-4-piperidyl]ethanol, prepared in step 2.1, in 30 ml of dichloromethane. The reaction mixture is then refluxed for 5 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08034818B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-e0dfc1e2180d4746b2b97d26068dc61c |
| Source note | uspto-grants-2011_10 |