HRID1663089

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID8359

2H-3,1-Benzoxazine-2,4(1H)-dione

C8H5NO3

HCID74168

Imidazole-1-ethanol

C5H8N2O

PRODUCTS

生成物

HCID58989834

未命名化合物

PROCEDURE

实验过程

Prepared by a similar procedure as described for preparation 7B, starting from isatoic anhydride and 1-(2-hydroxyethyl)-imidazole (Fluorochem). 13C-NMR (DMSO-d6) δ 158.7, 147.5, 141.3, 137.6, 136.9, 129.4, 128.5, 123.6, 119.7, 114.0, 111.3, 45.1, 43.3.

WORKUP

后处理

customPrepared by a similar procedure