HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isatoic Anhydride → 1-(2-Imidazol-1-yl-ethyl)-1H-benzo[d][1,3]oxazine-2,4-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isatoic Anhydride | HCID 8359 | — |
| Reactant | N-(2-Hydroxyethyl)imidazole | HCID 74168 | — |
| Product | 1-(2-Imidazol-1-yl-ethyl)-1H-benzo[d][1,3]oxazine-2,4-dione | HCID 58989834 | — |
Reaction Steps
Prepared by a similar procedure as described for preparation 7B, starting from isatoic anhydride and 1-(2-hydroxyethyl)-imidazole (Fluorochem). 13C-NMR (DMSO-d6) δ 158.7, 147.5, 141.3, 137.6, 136.9, 129.4, 128.5, 123.6, 119.7, 114.0, 111.3, 45.1, 43.3.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08034811B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-e37cc434d9e54f7ab349a427d0a909c6 |
| Source note | uspto-grants-2011_10 |