huagongshe.com
HRID1663094

反应详情

EQUATION

反应方程式

HRID 1663094 的结构方程式

REACTANTS

反应物

2
结构：Clc1ccc(CBr)cc1
HCID69329

1-(Bromomethyl)-4-chlorobenzene

C7H6BrCl

结构：CC(C)(C)OC(=O)NO
HCID97534

tert-Butyl N-hydroxycarbamate

C5H11NO3

PRODUCTS

生成物

1
结构：Cl.NOCc1ccc(Cl)cc1
HCID217573

O-[(4-Chlorophenyl)methyl]hydroxylamine--hydrogen chloride (1/1)

C7H9Cl2NO

PROCEDURE

实验过程

Same procedure as described for preparation 8. Starting materials: 4-Chlorobenzyl bromide and tert-butyl-N-hydroxycarbamate. 1H-NMR (DMSO-d6) δ 11.18 (bs, 3H), 7.44-7.51 (m, 4H), 5.06 (s, 2H).

WORKUP

后处理

  1. customSame procedure as described for preparation 8