N-Hydroxyphthalimide → HCID 67132065, compound

HRID 1663102Notes

Reaction equation

HRID 1663102 reaction equation
[OH:1][N:2]1C(=O)C2=CC=CC=C2C1=O.[Cl:13][CH2:14][C:15]1[CH:22]=[CH:21][C:18]([CH2:19][OH:20])=[CH:17][CH:16]=1>>[ClH:13].[NH2:2][O:1][CH2:14][C:15]1[CH:22]=[CH:21][C:18]([CH2:19][OH:20])=[CH:17][CH:16]=1

Participants

3

Reactant 2

HCID 10665N-HydroxyphthalimideHCID 5107660[4-(Chloromethyl)phenyl]methanol

Product 1

HCID 67132065HCID 67132065, compound

Procedure

Prepared by a similar procedure as described for preparation 18, starting from N-hydroxyphthalimide and 4-(chloromethyl)benzyl alcohol (Aldrich). 13C-NMR (DMSO-d6) δ 143.6, 131.8, 129.0, 126.4, 75.5, 62.4.

Workup

  1. customPrepared by a similar procedure
  2. customas described for preparation 18

Sources & evidence

ORD record
ord-4749afd038a747149ddd2ce665a66b85
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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