N-Hydroxyphthalimide → HCID 18525983, compound

HRID 1663104Notes

Reaction equation

HRID 1663104 reaction equation
[OH:1][N:2]1C(=O)C2=CC=CC=C2C1=O.[CH3:13][O:14][C:15]1[CH:22]=[CH:21][CH:20]=[CH:19][C:16]=1[CH2:17][Cl:18]>>[ClH:18].[CH3:13][O:14][C:15]1[CH:22]=[CH:21][CH:20]=[CH:19][C:16]=1[CH2:17][O:1][NH2:2]

Participants

3

Reactant 2

HCID 10665N-HydroxyphthalimideHCID 814952-(Chloromethyl)anisole

Product 1

HCID 18525983HCID 18525983, compound

Procedure

Prepared by a similar procedure as described for preparation 18, starting from N-hydroxyphthalimide and 2-methoxybenzyl chloride (Aldrich). 13C-NMR (DMSO-d6) δ 157.5, 130.8, 130.7, 121.5, 120.3, 111.1, 70.8, 55.4.

Workup

  1. customPrepared by a similar procedure
  2. customas described for preparation 18

Sources & evidence

ORD record
ord-3017402a84b341a79f329a06faf296b5
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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