N-Hydroxyphthalimide → HCID 24192743, compound

HRID 1663107Notes

Reaction equation

HRID 1663107 reaction equation
[OH:1][N:2]1C(=O)C2=CC=CC=C2C1=O.[CH2:13]1[O:17][C:16]2[CH:18]=[C:19]([Cl:24])[C:20]([CH2:22][Cl:23])=[CH:21][C:15]=2[O:14]1>>[ClH:23].[Cl:24][C:19]1[C:20]([CH2:22][O:1][NH2:2])=[CH:21][C:15]2[O:14][CH2:13][O:17][C:16]=2[CH:18]=1

Participants

3

Reactant 2

HCID 10665N-HydroxyphthalimideHCID 901136-Chloropiperonyl chloride

Product 1

HCID 24192743HCID 24192743, compound

Procedure

Prepared by a similar procedure as described for preparation 18, starting from N-hydroxyphthalimide and 6-chloropiperonyl chloride (Aldrich). 13C-NMR (DMSO-d6) δ 148.9, 146.5, 126.2, 124.2, 111.1, 109.8, 102.3, 72.7.

Workup

  1. customPrepared by a similar procedure
  2. customas described for preparation 18

Sources & evidence

ORD record
ord-e1a3aa7976334ecbb4ec1f2c929ace58
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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