N-Hydroxyphthalimide → HCID 22419624, compound

HRID 1663108Notes

Reaction equation

HRID 1663108 reaction equation
[OH:1][N:2]1C(=O)C2=CC=CC=C2C1=O.[CH2:13]1[O:23][C:22]2[CH:21]=[CH:20][C:17]([CH2:18]Cl)=[CH:16][C:15]=2[O:14]1>>[O:23]1[C:22]2[CH:21]=[CH:20][C:17]([CH2:18][O:1][NH2:2])=[CH:16][C:15]=2[O:14][CH2:13]1

Participants

3

Reactant 2

HCID 10665N-HydroxyphthalimideHCID 887131,3-Benzodioxole, 5-(chloromethyl)-

Product 1

HCID 22419624HCID 22419624, compound

Procedure

Prepared by a similar procedure as described for preparation 15, starting from N-hydroxyphthalimide and 3,4-methylenedioxybenzyl chloride (Fluorochem). 13C-NMR (CDCl3) δ 147.5, 147.2, 131.0, 121.9, 108.7, 107.9, 100.8, 77.5.

Workup

  1. customPrepared by a similar procedure
  2. customas described for preparation 15

Sources & evidence

ORD record
ord-69866a107c2a4ccea86ce8dc39ce6283
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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