N-Hydroxyphthalimide → HCID 25137652, compound

HRID 1663109Notes

Reaction equation

HRID 1663109 reaction equation
[OH:1][N:2]1C(=O)C2=CC=CC=C2C1=O.Br[CH2:14][C:15]1[CH:16]=[C:17]([CH:20]=[CH:21][CH:22]=1)[C:18]#[N:19]>>[NH2:2][O:1][CH2:14][C:15]1[CH:16]=[C:17]([CH:20]=[CH:21][CH:22]=1)[C:18]#[N:19]

Participants

3

Reactant 2

HCID 10665N-HydroxyphthalimideHCID 97249Benzonitrile, 3-(bromomethyl)-

Product 1

HCID 25137652HCID 25137652, compound

Procedure

Prepared by a similar procedure as described for preparation 15, starting from N-hydroxyphthalimide and 3-bromomethyl-benzonitrile. 13C-NMR (CDCl3) δ 139.5, 132.5, 131.7, 131.5, 129.2, 118.7, 112.6, 76.5.

Workup

  1. customPrepared by a similar procedure
  2. customas described for preparation 15

Sources & evidence

ORD record
ord-061ec13c77504e28946d51f04631b56e
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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