N-Hydroxyphthalimide → HCID 25137653, compound

HRID 1663110Notes

Reaction equation

HRID 1663110 reaction equation
O[N:2]1[C:6](=[O:7])[C:5]2=[CH:8][CH:9]=[CH:10][CH:11]=[C:4]2[C:3]1=O.BrCC1C=CC=CC=1C#[N:18]>>[NH2:18][O:7][CH2:6][C:5]1[CH:8]=[CH:9][CH:10]=[CH:11][C:4]=1[C:3]#[N:2]

Participants

3

Reactant 2

HCID 10665N-HydroxyphthalimideHCID 895992-(Bromomethyl)benzonitrile

Product 1

HCID 25137653HCID 25137653, compound

Procedure

Prepared by a similar procedure as described for preparation 15, starting from N-hydroxyphthalimide and 2-bromomethyl-benzonitrile. 13C-NMR (CDCl3) δ 141.3, 132.9, 132.8, 129.5, 128.4, 117.5, 112.4, 75.3

Workup

  1. customPrepared by a similar procedure
  2. customas described for preparation 15

Sources & evidence

ORD record
ord-b7b090cab13b4886b19cfb06fada79de
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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