N-Hydroxyphthalimide → O-(2-Amino-benzyl)-hydroxylamine

HRID 1663111Notes

Reaction equation

HRID 1663111 reaction equation
[NH2:1][C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[CH2:4][OH:5].O[N:11]1C(=O)C2=CC=CC=C2C1=O>>[NH2:1][C:2]1[CH:9]=[CH:8][CH:7]=[CH:6][C:3]=1[CH2:4][O:5][NH2:11]

Participants

3

Reactant 2

HCID 10665N-HydroxyphthalimideHCID 214392-Aminobenzyl alcohol

Product 1

HCID 25137659O-(2-Amino-benzyl)-hydroxylamine

Procedure

Prepared by a similar procedure as described for preparation 31 starting from 2-amino-benzylalcohol and N-hydroxyphthalimide. 13C-NMR (CDCl3) δ 146.4, 131.2, 129.7, 121.4, 118.1, 115.9, 76.6.

Workup

  1. customPrepared by a similar procedure

Sources & evidence

ORD record
ord-b53df15945694793bc6c5c6cc878471d
Source dataset
uspto-grants-2011_10
Patent number
US08034811B2

Reaction notes

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