HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Hydroxyphthalimide → O-[(3,5-Dimethyl-1,2-oxazol-4-yl)methyl]hydroxylamine--hydrogen chloride (1/1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Hydroxyphthalimide | HCID 10665 | — |
| Reactant | Isoxazole, 4-(chloromethyl)-3,5-dimethyl- | HCID 88246 | — |
| Product | O-[(3,5-Dimethyl-1,2-oxazol-4-yl)methyl]hydroxylamine--hydrogen chloride (1/1) | HCID 19974948 | — |
Reaction Steps
Prepared by a similar procedure as described for preparation 13. Starting materials: N-hydroxyphthalimide and 4-(chloromethyl)-3,5-dimethylisoxazole (Aldrich). 13C-NMR (DMSO-d6) δ 169.7, 159.6, 108.2, 64.4, 10.8, 9.5.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08034811B2 |
| Source dataset | uspto-grants-2011_10 |
| ORD ID | ord-ea2af63e688d4c47bac688bbdd909134 |
| Source note | uspto-grants-2011_10 |